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Development of conversion of biomass derivatives in combination with utilization of solar energy by photocatalysts is a promising alternative strategy for biorefineries. The photocatalytic reaction could convert glucose to a mixture of value-added chemicals under UV irradiation. Modifications of titanium dioxide (TiO2) nanoparticles by metal or metalloid (i.e., B and Ag) and nonmetal (i.e., N) dopants were carried out. The effects of co-doping (i.e., B/N and Ag/N) on physicochemical characteristics of the modified photocatalysts, photocatalytic glucose conversion, and the yields of the target chemical products (i.e., gluconic acid, xylitol, arabinose, and formic acid) were studied. The doping of the photocatalysts by different single dopants could improve the performance in terms of productivity and was further enhanced by the synergism from co-doping. The improvement in catalytic performances of the photocatalysts corresponded with the alterations in physicochemical characteristics of the catalysts resulting from the dopants.
Lignocellulose is a promising raw material for the production of second-generation biofuels. In this study, the effects of acid-catalyzed liquid hot water (LHW) on pretreatment of corn stover (CS) for subsequent hydrolysis and conversion to ethanol were studied. The effects of reaction temperature, acid concentration, and residence time on glucose yield were evaluated using a response surface methodology. The optimal condition was 162.4 °C for 29.5 min with 0.45% v/v of sulfuric acid, leading to the maximum glucose yield of 91.05% from enzymatic hydrolysis of the cellulose-enriched fraction. Conversion of the solid fraction to ethanol by simultaneous saccharification and fermentation resulted in a theoretical ethanol yield of 93.91% based on digestible glucose. Scanning electron microscopy revealed disruption on the microstructure of the pretreated CS. Increases of crystallinity index and surface area of the pretreated biomass were observed along with alteration in the functional group profiles, as demonstrated by Fourier transform infrared spectroscopy. This work provides an insight into the effects of LHW on the enzymatic susceptibility and modification of the physicochemical properties of CS for further application on bioethanol production in biorefinery.
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