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SrZrO3/flower-like MoS2 composites with an embedded heterostructure were synthesized via a simple two-step hydrothermal method and their performance was evaluated by photodegradation of methylene blue (MB) under solar-simulated light irradiation. The sandwiched flower-like MoS2 with a high Mo(VI) ratio was adopted as the matrix, and SrZrO3 was grown between the MoS2 layers, forming an intense contact interface, which promotes the efficient separation and transport of photoinduced carriers. The enhanced photocatalytic degradation of 99.7% after 80 min of irradiation is exhibited over the MS5 sample (5 wt % SrZrO3 loading amount on the MoS2 matrix). Moreover, the ratio of Mo(VI) and the superoxide radical plays a crucial role in the photodegradation of MB, and the higher the ratio the better the performance. This work provided a strategy to design a new kind of photocatalyst for photocatalysis and indicated that MoS2 is preferably adopted as a matrix rather than as a loading component.
A simple, in situ, and one-pot hydrothermal strategy was applied for the successful manufacturing of heterostructured 2D/2D BiOCl/g-C3N4 photocatalysts, and outstanding photodegradation of Rhodamine B in the condition of visible-light irradiation over the composites emerged. The investigation of various BiOCl/g-C3N4 ratios influencing the activity implied that the optimized B2C1 (mole ratio of BiOCl/g-C3N4 with 2:1) exhibited the higher degradation efficiency than that of the rest of the composites, even higher than that of pure BiOCl and pure g-C3N4, which yielded over 90% in the initial 30 min and reached almost 100% during the whole 70 min irradiation process. Kinds of characterizations demonstrated that the enhancement of photodegradation performance was caused by the intimate contact between BiOCl and g-C3N4 to form the heterostructure, which could benefit the generation of abundant visible-light photoinduced carriers and help enhance their separation and then promote their transportation to the surface.
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